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eBay-Artikelnr.:157276739855
Artikelmerkmale
- Artikelzustand
- ISBN
- 9780849300196
Über dieses Produkt
Product Identifiers
Publisher
CRC Press LLC
ISBN-10
0849300193
ISBN-13
9780849300196
eBay Product ID (ePID)
1954176
Product Key Features
Number of Pages
704 Pages
Publication Name
Crc Handbook of Optical Resolutions Via Diastereomeric Salt Formation
Language
English
Publication Year
2001
Subject
Chemistry / Physical & Theoretical, Chemistry / Organic, Chemistry / General
Type
Textbook
Subject Area
Science
Format
Hardcover
Dimensions
Item Height
1.7 in
Item Weight
46.5 Oz
Item Length
10.2 in
Item Width
7 in
Additional Product Features
Intended Audience
Scholarly & Professional
LCCN
2001-035243
Dewey Edition
21
Illustrated
Yes
Dewey Decimal
541.2252
Table Of Content
INTRODUCTION BASIC CONCEPTS AND NOMENCLATURE OF STEREOCHEMISTRY Chirality, Enantiomers and Diastereomers Stereochemical Nomenclature Principles of Separation of Diastereomers and Enantiomers RESOLUTION BY FORMATION AND FRACTIONAL CRYSTALLISATION OF DIASTEREOMERIC SALTS The Concept of Resolvability Stoichiometry of Resolution Resolution with One Equivalent of Resolving Agent Resolution with Half Equivalent of Resolving Agent in Combination with an Achiral Additive Use of Half Molar Equivalent of Resolving Agent without an Achiral Additive Salt-Salt Resolution Resolution with the Enantiomer of the Resolving Agent Reciprocal Resolution Mutual Resolution Resolution with Difunctional Resolving Agents Resolution of Amphoteric Racemates Resolution by Salt Formation of Compounds Lacking Acidic or Basic Groups Asymmetric Transformations during Resolution by Salt Formation RESOLVING AGENTS Basic Resolving Agents Acidic Resolving Agents (Including Amino Acids) RESEARCH ON RESOLVING AGENTS Attempts to Devise A Generally Applicable Resolving Agent Correlation of the Efficiency of Resolution with the Structure of Racemate and Resolving Agent. Resolutions with a Derivative of the Racemate Resolutions with a Mixture of Structurally Similar Resolving Agents SELECTION OF THE RESOLVING AGENT SELECTION OF THE RESOLVING AGENT BY EXPERIMENTATION Selection of the Resolving Agent by Small-Scale Preliminary Preparative Experiments Selection of the Resolving Agent by Combined Application of Several Resolving Agents Selection of the Resolving Agent by Distillation Tests Selection of the Resolving Agent Based on the Principle of Maximum Similarity Selection of the Resolving Agent by Statistical Evaluation SELECTION OF A RESOLVING AGENT BASED ON THE DETERMINATION OF PHYSICO-CHEMICAL PARAMETERS Solubility Selection of a Resolving Agent Based on Melting Point Phase Diagrams of Diastereomeric Salt Pairs Calculation of Resolvability by DSC of a Mixture of Diastereomeric Salts Formed from the Racemate Determination of the Optical Rotation of Diastereomeric salts SELECTION OF THE RESOLVING AGENT BASED ON THEORETICAL CONSIDERATIONS RESOLUTION IN PRACTICE, SELECTION OF THE OPTIMAL PARAMETERS Reacting the Components Initiation of Crystallisation Role of Temperature in Resolution Further Purification of Diastereomeric Salts with the Aid of a Chiral Additive Recovery of the Components from the Diastereomeric Salts Upgrading of Optical Purity without a Chiral Additive (Enantiomeric Enrichment) ALTERNATIVE METHODS OF RESOLUTION BY DIASTEREOMERIC SALT FORMATION Classification of Alternative Resolution Processes by Type of Phase Transition Resolution by Distillation Resolution by Extraction Resolution by Supercritical Extraction Resolution by Sublimation Mechanical Separation of Diastereomeric Salt Mixtures DETAILED DESCRIPTIONS OF SELECTED RESOLUTIONS APPENDIX 1: Resolutions Ordered According to the Resolving Agent APPENDIX 2: Commercially Produced Resolving Agents and Optically Active Industrial Products which may be Eligible as Resolving Agents APPENDIX 3. Chiral Selective Chromatographic Analysis
Synopsis
Optically active compounds are gaining ever-increasing importance in organic chemistry, both in the academic and the industrial arenas. The rational synthesis of the growing number of chiral chemicals, drugs, and natural products demands efficient methods for producing these compounds in an enantiomerically, highly pure form. Despite the available alternative techniques, optical resolution via Diastereomeric salt formation remains the most widely used method of preparing pure enantiomers. The CRC Handbook of Optical Resolutions Via Diastereomeric Salt Formation is the first book to exclusively address this important organic chemical process. It provides fast, one-stop access to a wealth of information, including all of the available data on 100 resolving agents, a list of 500 optically active compounds available in bulk along with their suppliers, data on more than 3,500 resolutions, and 4,200 citations. This handbook helps answer virtually any question that may arise during the development of a new resolution process. Which resolving agent and solvent should I use under these conditions? How can I separate the diastereoisomers? How can I optimize a resolution process? How do I determine enantiomeric purity? Which supplier has the resolving agent I need? For a racemate already resolved, what were the resolving agent, solvent, and relevant citation? This is the first book to deal exclusively with all aspects of this important organic chemical process, both theoretical and practical. With an abundance of analyzed examples, this single, authoritative reference provides all of the information you need to perform, develop, and optimize optical resolutions via Diastereomeric salt formation, Roughly half of the several ten thousand pharmaceutical drugs currently known have a chiral structure. The need for drugs with fewer side effects and safer pesticides calls for efficient methods providing these compounds in enantiomerically highly pure forms. This is the first book to deal exclusively with all aspects, both theoretical and practical, of this important organic chemical process,. With an abundance of analyzed examples, this single book provides all of the information necessary to perform, develop, and optimize optical resolutions via diastereomeric salt formation, being still the most practical method to obtain enantiomerically pure products both on laboratory or industrial scale.
LC Classification Number
QD481.C73 2001
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Verkäuferbewertungen (2.329)
- 1***3 (33)- Bewertung vom Käufer.Letzte 6 MonateBestätigter KaufThe book arrived promptly, extremely well packed and in excellent condition. The book is as described looking clean and appearance is as good as new. This book offered me value for money and I look forward to reading it. No problems with ordering from the USA for delivery to the UK. An excellent book seller - I would certainly purchase from Huff Books again. Thank you.
- o***r (539)- Bewertung vom Käufer.Letzte 6 MonateBestätigter KaufPrompt and courteous reply to pre-purchase inquiry about packing. Book arrived promptly, securely packed, and in as-described condition. I'm happy with the purchase and recommend the seller.Not much of an engineer by stanley hooker 1984 (Nr. 156126254462)
- e***g (779)- Bewertung vom Käufer.Letzte 6 MonateBestätigter KaufVintage 1934 Hardcover book "They Built The West: An Epic of Rails and Cities" by Glenn Chesney Quiett was well priced, and was received in good condition as described in listing. It was well packed for protection durning transit, and shipped very fast. Definitely recommend this Seller A+++++1934 "They Built The West: An Epic of Rails and Cities" by Glenn Chesney Quiett (Nr. 155778032464)